粉体工学会誌
Online ISSN : 1883-7239
Print ISSN : 0386-6157
ISSN-L : 0386-6157
49 巻, 1 号
選択された号の論文の5件中1~5を表示しています
  • 佐藤 洋, 菅原 勝康
    2012 年 49 巻 1 号 p. 4-11
    発行日: 2012/01/10
    公開日: 2012/01/27
    ジャーナル フリー
    In a series of studies on fabrication of thick-film inorganic electroluminescence device by co-firing of multi-layers consisted of phosphor, dielectric materials, transparent electrode and back electrode, effects of calcination condition, microstructure changes of Ca0.997Pr0.002TiO3 films during calcination or sintering, and barium diffusion from dielectric material to (Ca1-xSrx)0.997Pr0.002TiO3 phosphor on the photoluminescence characteristics were investigated. The results showed that calcination temperature above 800℃ was necessary for the phosphor to suppress the crack and delamination caused by gas evolution and expansion during co-firing. The sintered films with dense and high crystallinity could be prepared by two steps heat treatment consisted of calcination and co-firing. It was also shown that chemical composition change and solid solution formation due to the barium diffusion to the phosphor during co-firing affected remarkably on the photoluminescence intensity. The combination of CaTiO3:Pr phosphor and BaTiO3 dielectric material was an appropriate system for the co-firing of thick films because of no barium diffusion and formation of solid solution. It was demonstrated that the inorganic electroluminescence device could be prepared with dense and high crystalline films by selecting the combination of phosphor and dielectric materials and controlling their calcination and sintering conditions.
  • 小池 好満, 河府 賢治, 越智 光昭
    2012 年 49 巻 1 号 p. 12-18
    発行日: 2012/01/10
    公開日: 2012/01/27
    ジャーナル フリー
    In this research, the effect of frictional resistance on pressure loss in horizontal plug conveying was investigated. As a result, the ratio of pressure drop by the frictional loss to total loss ranged 70-93% tested conditions. It is also found that wall pressure at the bottom of pipe becomes the maximum due to gravity action. Furthermore, the cross sectional pressure distribution was found to be related to the particle velocity, i.e. as particle velocity becomes larger, wall pressure in circumference direction comes to act equally. Additionally, it was shown experimental values on mean wall pressure approach theoretical value.
  • 小池 好満, 河府 賢治, 越智 光昭
    2012 年 49 巻 1 号 p. 19-25
    発行日: 2012/01/10
    公開日: 2012/01/27
    ジャーナル フリー
    Ultrasonic vibration was applied to plug conveying line, and pressure drop was measured. As a result, pressure drop became smaller linearly with increasing of ultrasonic amplitude regardless of particles and flow conditions. Therefore, ultrasonic can reduce the frictional resistance between particles and pipe wall. Additionally the wall pressure was measured by the button sensors, and relation of reduction effect and wall pressure was examined. Reduction effect becomes smaller as wall pressure becomes larger in spite of kinds of particle. Therefore, it is possible to predict the reduction effect by ultrasonic.
解説
  • 林 潤, 赤松 史光
    2012 年 49 巻 1 号 p. 26-34
    発行日: 2012/01/10
    公開日: 2015/08/26
    ジャーナル 認証あり
    The efficient flame assisted spray pyrolysis method by using flash boiling atomization under low-pressure condition was proposed. Methane-oxygen premixed flame was utilized as the heat source and the precursor water solution was sprayed at low-pressure field. The precursor water spray, which injected in low-pressure field, was secondary-atomized by flash boiling atomization. In order to investigate the effects of flash boiling atomization on the nanosized particle synthesis, the flashing spray was visualized, measured and analyzed by the Mie scattering method and PDA measurement. Furthermore, ZnO nanoparticles synthesized for investigating the effects of flash boiling atomization on the generated particles. It was found that the spray droplet was well atomized and dispersed when flash boiling occurred. In addition the size of synthesized particles became smaller under the conditions of high temperature and of low pressure.
解説 フロンティア研究シリーズ
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