The changes of properties of cooked rices (non-glutinous rice (Non-Glut.) and glutinous rice (Glut.)) during storage at 5 °C were studied in relation to the retrogradation of starch. The results were as follows :
1) The amount of water-soluble fraction of Glut. was larger than that of Non-Glut. The amount of total carbohydrate of the fraction of Non-Glut. firstly increased, showing the maximum value at 3 hr after the storage, and thereafter, continuously decreased. In the case of Glut., the amount of the carbohydrate was almost constant for 3 hr and thereafter decreased.
The molecular size distribution of the carbohydrates of these fractions was analyzed by GPC and pursued their changes with time.
2) During the storage, the degree of gelatinization of Glut. was usually higher than that of Non-Glut. At 3 hr after the storage, the degree of gelatinization of Non-Glut. reached maximum value and decreased, while that of Glut. gradually decreased from the beginning.
3) X-ray diffraction patterns of both Non-Glut. and Glut. were changed from A type to V type by cooking. The V type pattern of Non-Glut. was characterized by the presence of a few helical complex of amylose and fatty acids and that of Glut. was of completely amorphous. Crystalline structures were partially recovered at 24 hr after the storage and B type patterns were apparently appeared after 144 hr.
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