Journal of Environmental Conservation Engineering
Online ISSN : 1882-8590
Print ISSN : 0388-9459
ISSN-L : 0388-9459
Volume 47, Issue 5
Displaying 1-3 of 3 articles from this issue
  • Koji FURUKAWA, Toshiyuki KAWAGUCHI, Kiyonobu KUDO, Tomoko NAKAZAWA, Ry ...
    2018 Volume 47 Issue 5 Pages 278-285
    Published: July 20, 2018
    Released on J-STAGE: July 27, 2018
    JOURNAL FREE ACCESS

    In this study, an analysis was conducted for the simultaneous determination method of aniline and quinoline in drinking water using liquid chromatography/tandem mass spectrometry.

    The calibration curves of aniline and quinoline, obtained from the results of the study, demonstrated good linearity in the range of 1.0 to 20 μg/L of aniline standard and in the range of 0.01 to 0.020 μg/L of quinolone standard. The repeatability of repeated measurements of aniline standard solution (0.02 μg/L, n=5) was observed to be below 0.82% and the repeatability of repeated measurements of quinoline standard solution (0.02 μg/L, n=5) was observed to be below 2.7%. In addition, the repeatability (4.8-5.6%), intermediate precision (4.8-12%), and accuracy (98.8-107%) values obtained via recovery tests for aniline and quinoline in drinking water (aniline: 1.0 μg/L, and quinoline: 0.01 μg/L, n=5, 5days) satisfied the criteria provided in the guidelines for the validation of testing methods for drinking water notified by the Ministry of Health, Labour and Welfare, Japan.

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