Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)
Online ISSN : 1882-1006
Print ISSN : 0015-6426
ISSN-L : 0015-6426
Volume 64, Issue 3
Displaying 1-3 of 3 articles from this issue
Notes
  • Keiko Iwakoshi, Katsushi Iwakoshi, Megumi Hasebe, Asa Osuga, Hiroyuki ...
    2023 Volume 64 Issue 3 Pages 101-107
    Published: June 25, 2023
    Released on J-STAGE: June 28, 2023
    JOURNAL RESTRICTED ACCESS
    Supplementary material

    Migrants found in migration solutions obtained from commercially available polyethylene products that may contain food were studied and analysed via liquid chromatography coupled with quadrupole time-of-flight mass spectrometry (LC-QTOF) for non-target screening and LC-MS/MS for quantifying 14 substances in migration solutions. Furthermore, an analytical approach based on the retention gap was developed for accurate separation techniques using LC-MS/MS. Irganox 1076 was detected at a maximum of 1.5 mg/kg, which was 1/4 of the Specific Migration Limit in the EU, in nine commercially available plastic bags tested. This is in accordance with European Regulation No 10/2011/EU. Furthermore, migration of Erucamide and Irgafos 168-oxide was confirmed.

    Download PDF (451K)
  • Hideyuki Shinohara, Ryuma Okawara, Yuka Nagaoka
    2023 Volume 64 Issue 3 Pages 108-110
    Published: June 25, 2023
    Released on J-STAGE: June 28, 2023
    JOURNAL RESTRICTED ACCESS

    A simple method of identification using a color reaction was developed for Omphalotus guepiniformis. Only Omphalotus guepiniformis turned turquoise green. Other edible mushrooms resembling the mushroom did not change color when the beam reagent (5 w/v% potassium hydroxide ethanolic solution) was dripped onto the mushroom pileus. Furthermore, ethanol extract and mock cooking products of this mushroom exhibited the same color reaction. These results demonstrate this method as useful for identifying Omphalotus guepiniformis during mushroom hunting or during investigations of food poisoning.

    Download PDF (1741K)
Validation Study
  • Yohei Kataoka, Motoh Mutsuga, Yutaka Abe, Midori Kondo, Michiyo Yotsuy ...
    2023 Volume 64 Issue 3 Pages 111-115
    Published: June 25, 2023
    Released on J-STAGE: June 28, 2023
    JOURNAL RESTRICTED ACCESS
    Supplementary material

    A validation study was performed on the modified analytical method for the migration solution of heptane, 20% ethanol and 4% acetic acid for the determination of bisphenol A migrating from polycarbonate food apparatuses, containers, and packaging. The analytes for the method were bisphenol A, phenol and p-tert-butylphenol. The repeatability, within-laboratory reproducibility and trueness of the method was estimated in the range of 0.2–1.8%, 0.4–2.6% and 95–102% respectively. These results showed that the method is useful as an analytical method for the migration solution of heptane, 20% ethanol and 4% acetic acid. Furthermore, the applicability of the determination methods with a fluorescence detector was verified. As a result of the validation study, the repeatability, within-laboratory reproducibility and trueness of the method was estimated in the range of 0.1–2.9%, 0.2–3.1% and 94–101% respectively. It was confirmed that the measurement with a fluorescence detector is also available.

    Download PDF (483K)
feedback
Top