Discharge characteristics at 1 MHz in CF
4/O
2 mixture at the total pressure of 66.5 Pa (0.5 Torr) have been investigated by electrical and optical methods. The discharge parameters such as the discharge-sustaining voltage and the discharge current in CF
4/O
2 discharge vary synergistically as a function of the gas mixing ratio. As mixing CF
4 gas with O
2 gas, the discharge mode varies from hollow plasma distribution in O
2 discharge to uniform one in CF
4/O
2 discharge. In a range of CF
4 ratio from 50 to 95%, the electron temperature increases over that in O
2 discharge, and furthermore the intense photo-emission in front of the instantaneous anode due to the double layer is observed around the phases of ωt =π/2 and 3π/2. This emission profile is similar to that in strong electronegative SF
6 discharge. These findings seem to come from the enhancement of electronegativity in CF
4/O
2 discharge at large CF
4 mixting ratio.
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